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(1) Where applicable, custom lab flags have been used on this report; V = surrogate recovery is not within method/contract control limits. <br />(2) R(%) = percent recovery. <br />These data are validated and reported as accurate and in accord with SGS AXYS Analytical Services Ltd. ISO17025 compliant quality assurance <br />processes. <br />Signed: ___________Bryan Alonzo___________ <br />For Axys Internal Use Only [ XSL Template: FC-Form2.xsl; Created: 16-Jun-2020 11:23:07; Application: XMLTransformer-1.18.7; <br />Report Filename: PFC_FC_LC_PFAS_L33032-2_Form2_FC0L_151S21_SJ2745754.html; Workgroup: WG72387; Design ID: 3973 ] <br />SGS AXYS METHOD MLA-110 Rev 02 CLIENT SAMPLE NO. <br />Lino Lakes Well No.3 <br />Sample Collection: <br />05-May-2020 11:00 <br />Form 2 <br />PERFLUORINATED ORGANICS ANALYSIS REPORT <br />SGS AXYS ANALYTICAL SERVICES <br />2045 MILLS RD., SIDNEY, B.C., CANADA <br />V8L 5X2 TEL (250) 655-5800 FAX (250) 655-5811 <br />Project No.LINO LAKES WTP FEASIBILITY <br />015822-000 <br />Contract No.:5036 Lab Sample I.D.:L33032-2 <br />Matrix:AQUEOUS Sample Size:0.547 L <br />Sample Receipt Date:06-May-2020 Initial Calibration Date:18-Mar-2020 <br />Extraction Date:15-May-2020 Instrument ID:LCMS/MS <br />Analysis Date:15-May-2020 Time:21:40:21 Column ID:C18 <br />Extract Volume (uL):4000 Sample Data Filename:FC0L_151 S: 21 <br />Injection Volume (uL):2 Blank Data Filename:FC0L_151 S: 19 <br />Dilution Factor:N/A Cal. Ver. Data Filename:FC0L_151 S: 12 <br />Concentration Units:ng absolute <br />This page is part of a total report that contains information necessary for accreditation compliance. <br />Results are compliant with NELAP accreditation described in the total report. Sample results relate only to the sample tested. <br />LABELED COMPOUND LAB <br />FLAG 1 <br />SPIKE <br />CONC. <br />CONC. <br />FOUND R(%)2 RETENTION <br />TIME <br />13C4-PFBA 40.0 26.0 64.9 1:55 <br />13C5-PFPeA 20.0 18.0 90.0 4:21 <br />13C5-PFHxA 10.0 9.01 90.1 4:56 <br />13C4-PFHpA 10.0 8.56 85.6 5:24 <br />13C8-PFOA 10.0 8.49 84.9 6:10 <br />13C9-PFNA 5.00 3.98 79.6 7:01 <br />13C6-PFDA 5.00 4.18 83.6 7:30 <br />13C7-PFUnA 5.00 4.01 80.2 7:50 <br />13C2-PFDoA 5.00 4.03 80.6 8:06 <br />13C2-PFTeDA 5.00 3.14 62.8 8:52 <br />13C3-PFBS 10.0 8.99 89.9 4:53 <br />13C3-PFHxS 10.0 8.34 83.4 6:17 <br />13C8-PFOS 10.0 8.78 87.8 7:36 <br />13C2-4:2 FTS 20.0 12.4 62.1 4:49 <br />13C2-6:2 FTS 20.0 12.1 60.6 5:51 <br />13C2-8:2 FTS 20.0 13.0 64.9 7:21 <br />13C8-PFOSA 10.0 8.84 88.4 8:43 <br />D3-N-MeFOSA 10.0 8.60 86.0 10:07 <br />D5-N-EtFOSA 10.0 7.65 76.5 10:24 <br />D3-MeFOSAA 20.0 11.3 56.7 7:33 <br />D5-EtFOSAA V 20.0 9.42 47.1 7:42 <br />d7-NMe-FOSE 100 70.7 70.7 9:59 <br />d9-NEt-FOSE 100 65.2 65.2 10:16 <br />13C3-HFPO-DA 40.0 33.4 83.6 5:05 <br />Page 1 of 1 (WG72387 -PFC_FC_LC_PFAS_L33032-2_Form2_FC0L_151S21_SJ2745754.html) <br />www.axysanalytical.com <br />Page 39 of 94