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QC Sample Results Job ID: 310-229849-1Client: WSB & Associates, Inc Project/Site: Kenzie Terrace Method: 8260D - Volatile Organic Compounds by GC/MS (Continued) Client Sample ID: Method BlankLab Sample ID: MB 310-351212/5 Matrix: Water Prep Type: Total/NA Analysis Batch: 351212 RL MDL Dichloropropane, 1,2-<1.00 1.00 ug/L 04/27/22 21:29 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier <1.00 1.00 ug/L 04/27/22 21:29 1Dichloropropane, 1,3- <4.00 4.00 ug/L 04/27/22 21:29 1Dichloropropane, 2,2- <1.00 1.00 ug/L 04/27/22 21:29 1Dichloropropene, 1,1- <5.00 5.00 ug/L 04/27/22 21:29 1Dichloropropene, cis 1,3- <5.00 5.00 ug/L 04/27/22 21:29 1Dichloropropene, trans 1,3- <2.00 2.00 ug/L 04/27/22 21:29 1Diethyl ether <1.00 1.00 ug/L 04/27/22 21:29 1Ethylbenzene <5.00 5.00 ug/L 04/27/22 21:29 1Hexachlorobutadiene <1.00 1.00 ug/L 04/27/22 21:29 1Isopropylbenzene <1.00 1.00 ug/L 04/27/22 21:29 1p-Isopropyltoluene <10.0 10.0 ug/L 04/27/22 21:29 1Methyl ethyl ketone (MEK) <10.0 10.0 ug/L 04/27/22 21:29 14-Methyl-2-pentanone (MIBK) <1.00 1.00 ug/L 04/27/22 21:29 1Methyl tert-butyl ether <5.00 5.00 ug/L 04/27/22 21:29 1Naphthalene <1.00 1.00 ug/L 04/27/22 21:29 1Propylbenzene, n- <1.00 1.00 ug/L 04/27/22 21:29 1Styrene <1.00 1.00 ug/L 04/27/22 21:29 11,1,1,2-Tetrachloroethane <1.00 1.00 ug/L 04/27/22 21:29 11,1,2,2-Tetrachloroethane <1.00 1.00 ug/L 04/27/22 21:29 1Tetrachloroethene <10.0 10.0 ug/L 04/27/22 21:29 1Tetrahydrofuran <1.00 1.00 ug/L 04/27/22 21:29 1Toluene <5.00 5.00 ug/L 04/27/22 21:29 11,2,3-Trichlorobenzene <5.00 5.00 ug/L 04/27/22 21:29 11,2,4-Trichlorobenzene <1.00 1.00 ug/L 04/27/22 21:29 11,1,1-Trichloroethane <1.00 1.00 ug/L 04/27/22 21:29 11,1,2-Trichloroethane <1.00 1.00 ug/L 04/27/22 21:29 1Trichloroethene <4.00 4.00 ug/L 04/27/22 21:29 1Trichlorofluoromethane <1.00 1.00 ug/L 04/27/22 21:29 11,2,3-Trichloropropane <2.00 2.00 ug/L 04/27/22 21:29 11,1,2-Trichlorotrifluoroethane <1.00 1.00 ug/L 04/27/22 21:29 11,2,4-Trimethylbenzene <1.00 1.00 ug/L 04/27/22 21:29 11,3,5-Trimethylbenzene <1.00 1.00 ug/L 04/27/22 21:29 1Vinyl chloride <3.00 3.00 ug/L 04/27/22 21:29 1Xylenes, Total 4-Bromofluorobenzene (Surr)98 80 -120 04/27/22 21:29 1 MB MB Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery 102 04/27/22 21:29 1Dibromofluoromethane (Surr)79 -120 105 04/27/22 21:29 1Toluene-d8 (Surr)79 -120 Client Sample ID: Lab Control SampleLab Sample ID: LCS 310-351212/6 Matrix: Water Prep Type: Total/NA Analysis Batch: 351212 Acetone 40.0 41.24 ug/L 103 50 -150 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits Allyl chloride 20.0 16.97 ug/L 85 49 -150 Benzene 20.0 20.14 ug/L 101 73 -127 Eurofins Cedar Falls Page 60 of 90 5/17/2022 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15