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QC Sample Results <br />Job ID: 310-229849-1Client: WSB & Associates, Inc <br />Project/Site: Kenzie Terrace <br />Method: 8260D - Volatile Organic Compounds by GC/MS (Continued) <br />Client Sample ID: Matrix Spike DuplicateLab Sample ID: 310-229839-B-26 MSD <br />Matrix: Water Prep Type: Total/NA <br />Analysis Batch: 351212 <br />Naphthalene <5.00 25.0 22.76 ug/L 91 37 -150 6 29 <br />Analyte <br />MSD MSD <br />DUnitResultQualifier %Rec <br />Spike <br />Added <br />Sample <br />Result <br />Sample <br />Qualifier <br />%Rec <br />Limits LimitRPD <br />RPD <br />Propylbenzene, n-<1.00 25.0 22.39 ug/L 90 37 -135 3 21 <br />Styrene <1.00 25.0 21.48 ug/L 86 44 -138 0 22 <br />1,1,1,2-Tetrachloroethane <1.00 25.0 22.07 ug/L 88 45 -140 0 23 <br />1,1,2,2-Tetrachloroethane <1.00 25.0 22.15 ug/L 89 51 -140 2 22 <br />Tetrachloroethene <1.00 25.0 19.11 ug/L 76 43 -135 1 23 <br />Tetrahydrofuran <10.0 50.0 46.45 ug/L 93 44 -150 5 25 <br />Toluene <1.00 25.0 20.16 ug/L 81 44 -136 2 22 <br />1,2,3-Trichlorobenzene <5.00 25.0 23.10 ug/L 92 37 -150 6 24 <br />1,2,4-Trichlorobenzene <5.00 25.0 22.06 ug/L 88 38 -135 6 21 <br />1,1,1-Trichloroethane <1.00 25.0 21.34 ug/L 85 52 -129 0 22 <br />1,1,2-Trichloroethane <1.00 25.0 20.92 ug/L 84 50 -142 1 24 <br />Trichloroethene <1.00 25.0 20.99 ug/L 84 49 -130 1 21 <br />1,2,3-Trichloropropane <1.00 25.0 22.27 ug/L 89 49 -146 3 32 <br />1,1,2-Trichlorotrifluoroethane <2.00 25.0 17.08 ug/L 68 42 -142 3 26 <br />1,2,4-Trimethylbenzene <1.00 25.0 21.96 ug/L 88 37 -142 4 25 <br />1,3,5-Trimethylbenzene <1.00 25.0 22.42 ug/L 90 39 -142 2 20 <br />Xylenes, Total <3.00 50.0 46.48 ug/L 93 40 -140 2 23 <br />4-Bromofluorobenzene (Surr)80 -120 <br />Surrogate <br />97 <br />MSD MSD <br />Qualifier Limits%Recovery <br />100Dibromofluoromethane (Surr)79 -120 <br />105Toluene-d8 (Surr)79 -120 <br />Method: WI-GRO - Wisconsin - Gasoline Range Organics (GC) <br />Client Sample ID: Method BlankLab Sample ID: MB 310-350984/5 <br />Matrix: Water Prep Type: Total/NA <br />Analysis Batch: 350984 <br />RL MDL <br />Wisconsin GRO <100 100 ug/L 04/26/22 04:37 1 <br />MB MB <br />Analyte Dil FacAnalyzedPreparedDUnitResultQualifier <br />4-Bromofluorobenzene (Surr)88 80 -120 04/26/22 04:37 1 <br />MB MB <br />Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery <br />Client Sample ID: Lab Control SampleLab Sample ID: LCS 310-350984/4 <br />Matrix: Water Prep Type: Total/NA <br />Analysis Batch: 350984 <br />Wisconsin GRO 800 834.3 ug/L 104 80 -120 <br />Analyte <br />LCS LCS <br />DUnitResultQualifier %Rec <br />Spike <br />Added <br />%Rec <br />Limits <br />4-Bromofluorobenzene (Surr)80 -120 <br />Surrogate <br />110 <br />LCS LCS <br />Qualifier Limits%Recovery <br />Eurofins Cedar Falls <br />Page 65 of 90 5/17/2022 <br />1 <br />2 <br />3 <br />4 <br />5 <br />6 <br />7 <br />8 <br />9 <br />10 <br />11 <br />12 <br />13 <br />14 <br />15