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QC Sample Results <br />Job ID: 310-229849-1Client: WSB & Associates, Inc <br />Project/Site: Kenzie Terrace <br />Method: 6020B - Metals (ICP/MS) (Continued) <br />Client Sample ID: Method BlankLab Sample ID: MB 310-351801/1-A ^5 <br />Matrix: Solid Prep Type: Total/NA <br />Analysis Batch: 353287 Prep Batch: 351801 <br />RL MDL <br />Silver <0.234 0.234 mg/Kg 05/03/22 10:30 05/16/22 19:29 5 <br />MB MB <br />Analyte Dil FacAnalyzedPreparedDUnitResultQualifier <br />Client Sample ID: Lab Control SampleLab Sample ID: LCS 310-351801/2-A ^20 <br />Matrix: Solid Prep Type: Total/NA <br />Analysis Batch: 353287 Prep Batch: 351801 <br />Arsenic 182 173.5 mg/Kg 95 80 -120 <br />Analyte <br />LCS LCS <br />DUnitResultQualifier %Rec <br />Spike <br />Added <br />%Rec <br />Limits <br />Barium 91.1 84.12 mg/Kg 92 80 -120 <br />Cadmium 91.1 86.83 mg/Kg 95 80 -120 <br />Chromium 91.1 84.21 mg/Kg 92 80 -120 <br />Lead 182 183.6 mg/Kg 101 80 -120 <br />Selenium 364 343.7 mg/Kg 94 80 -120 <br />Silver 91.1 96.27 mg/Kg 106 80 -120 <br />Client Sample ID: B-1 (20-22)Lab Sample ID: 310-229849-3 MS <br />Matrix: Solid Prep Type: Total/NA <br />Analysis Batch: 353287 Prep Batch: 351801 <br />Arsenic 4.72 173 188.0 mg/Kg 106 75 -125☼ <br />Analyte <br />MS MS <br />DUnitResultQualifier %Rec <br />Spike <br />Added <br />Sample <br />Result <br />Sample <br />Qualifier <br />%Rec <br />Limits <br />Barium 80.4 86.5 174.7 mg/Kg 109 75 -125☼ <br />Cadmium <0.445 86.5 90.57 mg/Kg 104 75 -125☼ <br />Chromium 15.4 86.5 103.1 mg/Kg 101 75 -125☼ <br />Lead 5.73 173 200.3 mg/Kg 113 75 -125☼ <br />Selenium <1.34 346 366.2 mg/Kg 106 75 -125☼ <br />Silver 0.252 86.5 101.3 mg/Kg 117 75 -125☼ <br />Client Sample ID: B-1 (20-22)Lab Sample ID: 310-229849-3 MSD <br />Matrix: Solid Prep Type: Total/NA <br />Analysis Batch: 353287 Prep Batch: 351801 <br />Arsenic 4.72 174 183.6 mg/Kg 103 75 -125 2 20☼ <br />Analyte <br />MSD MSD <br />DUnitResultQualifier %Rec <br />Spike <br />Added <br />Sample <br />Result <br />Sample <br />Qualifier <br />%Rec <br />Limits LimitRPD <br />RPD <br />Barium 80.4 87.0 162.2 mg/Kg 94 75 -125 7 20☼ <br />Cadmium <0.445 87.0 87.53 mg/Kg 100 75 -125 3 20☼ <br />Chromium 15.4 87.0 99.39 mg/Kg 96 75 -125 4 20☼ <br />Lead 5.73 174 191.1 mg/Kg 106 75 -125 5 20☼ <br />Selenium <1.34 348 358.7 mg/Kg 103 75 -125 2 20☼ <br />Silver 0.252 87.0 98.52 mg/Kg 113 75 -125 3 20☼ <br />Client Sample ID: Method BlankLab Sample ID: MB 310-351573/1-B <br />Matrix: Water Prep Type: Dissolved <br />Analysis Batch: 353287 Prep Batch: 351576 <br />RL MDL <br />Arsenic <2.00 2.00 ug/L 05/02/22 09:15 05/16/22 18:01 1 <br />MB MB <br />Analyte Dil FacAnalyzedPreparedDUnitResultQualifier <br /><2.00 2.00 ug/L 05/02/22 09:15 05/16/22 18:01 1Barium <br /><0.100 0.100 ug/L 05/02/22 09:15 05/16/22 18:01 1Cadmium <br /><5.00 5.00 ug/L 05/02/22 09:15 05/16/22 18:01 1Chromium <br />Eurofins Cedar Falls <br />Page 70 of 90 5/17/2022 <br />1 <br />2 <br />3 <br />4 <br />5 <br />6 <br />7 <br />8 <br />9 <br />10 <br />11 <br />12 <br />13 <br />14 <br />15