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Client Sample Results <br />Job ID: 310-229849-1Client: WSB & Associates, Inc <br />Project/Site: Kenzie Terrace <br />Lab Sample ID: 310-229849-8Client Sample ID: B-3 (20-22) <br />Matrix: SolidDate Collected: 04/22/22 14:00 <br />Date Received: 04/23/22 10:30 <br />Method: 8260D - Volatile Organic Compounds by GC/MS (Continued) <br />RL MDL <br />Styrene <0.138 0.138 mg/Kg ☼04/25/22 10:46 04/25/22 19:34 1 <br />Analyte Dil FacAnalyzedPreparedUnitDResultQualifier <br />0.138 mg/Kg 04/25/22 10:46 04/25/22 19:34 1☼1,1,1,2-Tetrachloroethane <0.138 <br />0.138 mg/Kg 04/25/22 10:46 04/25/22 19:34 1☼1,1,2,2-Tetrachloroethane <0.138 <br />0.138 mg/Kg 04/25/22 10:46 04/25/22 19:34 1☼Tetrachloroethene <0.138 <br />0.138 mg/Kg 04/25/22 10:46 04/25/22 19:34 1☼Tetrahydrofuran <0.138 <br />0.138 mg/Kg 04/25/22 10:46 04/25/22 19:34 1☼Toluene <0.138 <br />0.138 mg/Kg 04/25/22 10:46 04/25/22 19:34 1☼1,2,3-Trichlorobenzene <0.138 <br />0.138 mg/Kg 04/25/22 10:46 04/25/22 19:34 1☼1,2,4-Trichlorobenzene <0.138 <br />0.138 mg/Kg 04/25/22 10:46 04/25/22 19:34 1☼1,1,1-Trichloroethane <0.138 <br />0.138 mg/Kg 04/25/22 10:46 04/25/22 19:34 1☼1,1,2-Trichloroethane <0.138 <br />0.138 mg/Kg 04/25/22 10:46 04/25/22 19:34 1☼Trichloroethene <0.138 <br />0.138 mg/Kg 04/25/22 10:46 04/25/22 19:34 1☼Trichlorofluoromethane <0.138 <br />0.138 mg/Kg 04/25/22 10:46 04/25/22 19:34 1☼1,2,3-Trichloropropane <0.138 <br />0.138 mg/Kg 04/25/22 10:46 04/25/22 19:34 1☼1,1,2-Trichlorotrifluoroethane <0.138 <br />0.138 mg/Kg 04/25/22 10:46 04/25/22 19:34 1☼1,2,4-Trimethylbenzene <0.138 <br />0.138 mg/Kg 04/25/22 10:46 04/25/22 19:34 1☼1,3,5-Trimethylbenzene <0.138 <br />0.138 mg/Kg 04/25/22 10:46 04/25/22 19:34 1☼Vinyl chloride <0.138 <br />0.206 mg/Kg 04/25/22 10:46 04/25/22 19:34 1☼Xylenes, Total <0.206 <br />4-Bromofluorobenzene (Surr)105 79 -120 04/25/22 10:46 04/25/22 19:34 1 <br />Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery <br />Dibromofluoromethane (Surr)96 04/25/22 10:46 04/25/22 19:34 180-124 <br />Toluene-d8 (Surr)104 04/25/22 10:46 04/25/22 19:34 178-120 <br />Method: WI-GRO - Wisconsin - Gasoline Range Organics (GC) <br />RL MDL <br />Wisconsin GRO <9.87 9.87 mg/Kg ☼05/02/22 16:52 05/02/22 22:30 1 <br />Analyte Dil FacAnalyzedPreparedUnitDResultQualifier <br />4-Bromofluorobenzene (Surr)98 80 -120 05/02/22 16:52 05/02/22 22:30 1 <br />Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery <br />Method: WI-DRO - Wisconsin - Diesel Range Organics (GC) <br />RL MDL <br />Diesel Range Organics (DRO)<5.66 5.66 mg/Kg ☼04/25/22 08:58 04/25/22 17:01 1 <br />Analyte Dil FacAnalyzedPreparedUnitDResultQualifier <br />Method: 6020B - Metals (ICP/MS) <br />RL MDL <br />Arsenic 3.51 0.915 mg/Kg ☼05/03/22 10:30 05/16/22 20:26 5 <br />Analyte Dil FacAnalyzedPreparedUnitDResultQualifier <br />0.915 mg/Kg 05/03/22 10:30 05/16/22 20:26 5☼Barium 50.1 <br />0.458 mg/Kg 05/03/22 10:30 05/16/22 20:26 5☼Cadmium <0.458 <br />1.37 mg/Kg 05/03/22 10:30 05/16/22 20:26 5☼Chromium 9.58 <br />2.29 mg/Kg 05/03/22 10:30 05/16/22 20:26 5☼Lead 3.96 <br />1.37 mg/Kg 05/03/22 10:30 05/16/22 20:26 5☼Selenium <1.37 <br />0.229 mg/Kg 05/03/22 10:30 05/16/22 20:26 5☼Silver <0.229 <br />Method: 7471B - Mercury (CVAA) <br />RL MDL <br />Mercury 0.0192 0.0186 mg/Kg ☼04/29/22 12:14 05/02/22 14:12 1 <br />Analyte Dil FacAnalyzedPreparedUnitDResultQualifier <br />Eurofins Cedar Falls <br />Page 28 of 90 5/17/2022 <br />1 <br />2 <br />3 <br />4 <br />5 <br />6 <br />7 <br />8 <br />9 <br />10 <br />11 <br />12 <br />13 <br />14 <br />15