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QC Sample Results Job ID: 310-229849-1Client: WSB & Associates, Inc Project/Site: Kenzie Terrace Method: 8260D - Volatile Organic Compounds by GC/MS (Continued) Client Sample ID: Method BlankLab Sample ID: MB 310-350904/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 350927 Prep Batch: 350904 RL MDL Propylbenzene, n-<0.0991 0.0991 mg/Kg 04/25/22 10:46 04/25/22 13:52 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier <0.0991 0.0991 mg/Kg 04/25/22 10:46 04/25/22 13:52 1Styrene <0.0991 0.0991 mg/Kg 04/25/22 10:46 04/25/22 13:52 11,1,1,2-Tetrachloroethane <0.0991 0.0991 mg/Kg 04/25/22 10:46 04/25/22 13:52 11,1,2,2-Tetrachloroethane <0.0991 0.0991 mg/Kg 04/25/22 10:46 04/25/22 13:52 1Tetrachloroethene <0.0991 0.0991 mg/Kg 04/25/22 10:46 04/25/22 13:52 1Tetrahydrofuran <0.0991 0.0991 mg/Kg 04/25/22 10:46 04/25/22 13:52 1Toluene <0.0991 0.0991 mg/Kg 04/25/22 10:46 04/25/22 13:52 11,2,3-Trichlorobenzene <0.0991 0.0991 mg/Kg 04/25/22 10:46 04/25/22 13:52 11,2,4-Trichlorobenzene <0.0991 0.0991 mg/Kg 04/25/22 10:46 04/25/22 13:52 11,1,1-Trichloroethane <0.0991 0.0991 mg/Kg 04/25/22 10:46 04/25/22 13:52 11,1,2-Trichloroethane <0.0991 0.0991 mg/Kg 04/25/22 10:46 04/25/22 13:52 1Trichloroethene <0.0991 0.0991 mg/Kg 04/25/22 10:46 04/25/22 13:52 1Trichlorofluoromethane <0.0991 0.0991 mg/Kg 04/25/22 10:46 04/25/22 13:52 11,2,3-Trichloropropane <0.0991 0.0991 mg/Kg 04/25/22 10:46 04/25/22 13:52 11,1,2-Trichlorotrifluoroethane <0.0991 0.0991 mg/Kg 04/25/22 10:46 04/25/22 13:52 11,2,4-Trimethylbenzene <0.0991 0.0991 mg/Kg 04/25/22 10:46 04/25/22 13:52 11,3,5-Trimethylbenzene <0.0991 0.0991 mg/Kg 04/25/22 10:46 04/25/22 13:52 1Vinyl chloride <0.149 0.149 mg/Kg 04/25/22 10:46 04/25/22 13:52 1Xylenes, Total 4-Bromofluorobenzene (Surr)102 79 -120 04/25/22 13:52 1 MB MB Surrogate 04/25/22 10:46 Dil FacPreparedAnalyzedQualifierLimits%Recovery 98 04/25/22 10:46 04/25/22 13:52 1Dibromofluoromethane (Surr)80 -124 104 04/25/22 10:46 04/25/22 13:52 1Toluene-d8 (Surr)78 -120 Client Sample ID: Lab Control SampleLab Sample ID: LCS 310-350904/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 350927 Prep Batch: 350904 Acetone 1.99 2.015 mg/Kg 101 44 -150 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits Allyl chloride 0.995 1.017 mg/Kg 102 62 -150 Benzene 0.995 1.016 mg/Kg 102 80 -134 Bromobenzene 0.995 0.9577 mg/Kg 96 80 -126 Bromochloromethane 0.995 1.084 mg/Kg 109 80 -144 Bromodichloromethane 0.995 1.098 mg/Kg 110 75 -132 Bromoform 0.995 0.8492 mg/Kg 85 62 -131 Butylbenzene, n-0.995 0.9706 mg/Kg 98 75 -126 Butylbenzene, sec-0.995 0.9572 mg/Kg 96 79 -122 Butylbenzene, tert-0.995 0.9661 mg/Kg 97 79 -124 Carbon tetrachloride 0.995 1.058 mg/Kg 106 78 -132 Chlorobenzene 0.995 1.023 mg/Kg 103 80 -126 Chloroform 0.995 1.067 mg/Kg 107 80 -138 2-Chlorotoluene 0.995 1.036 mg/Kg 104 80 -126 4-Chlorotoluene 0.995 0.9943 mg/Kg 100 80 -125 Dibromo-3-chloropropane, 1,2-0.995 0.8067 mg/Kg 81 45 -145 Dibromochloromethane 0.995 0.9462 mg/Kg 95 74 -128 Dibromoethane, 1,2-0.995 1.030 mg/Kg 104 80 -128 Eurofins Cedar Falls Page 42 of 90 5/17/2022 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15