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QC Sample Results Job ID: 310-229849-1Client: WSB & Associates, Inc Project/Site: Kenzie Terrace Method: 8260D - Volatile Organic Compounds by GC/MS (Continued) Client Sample ID: Matrix Spike DuplicateLab Sample ID: 310-229044-B-1-H MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 350927 Prep Batch: 350904 Dichloroethylene, cis-1,2-<0.0982 0.976 0.8951 mg/Kg 92 53 -150 1 37 Analyte MSD MSD DUnitResultQualifier %Rec Spike Added Sample Result Sample Qualifier %Rec Limits LimitRPD RPD Dichloroethylene, trans-1,2 <0.0982 0.976 0.8351 mg/Kg 86 52 -150 4 33 Dichloromethane 0.355 0.976 1.134 mg/Kg 80 47 -150 9 32 Dichloropropane, 1,2-<0.0982 0.976 0.9649 mg/Kg 99 52 -150 2 38 Dichloropropane, 1,3-<0.0982 0.976 0.9274 mg/Kg 95 54 -150 4 37 Dichloropropane, 2,2-<0.0982 0.976 0.8372 mg/Kg 86 34 -150 2 33 Dichloropropene, 1,1-<0.0982 0.976 0.8863 mg/Kg 91 52 -150 3 38 Dichloropropene, cis 1,3-<0.0982 0.976 0.8696 mg/Kg 89 46 -150 3 39 Dichloropropene, trans 1,3-<0.0982 0.976 0.9142 mg/Kg 94 48 -150 5 39 Ethyl ether <0.0982 0.976 0.8687 mg/Kg 89 51 -150 2 35 Ethylbenzene <0.0982 0.976 0.8364 mg/Kg 86 34 -150 8 39 Hexachlorobutadiene <0.0982 0.976 0.7031 mg/Kg 72 22 -150 18 40 Isopropylbenzene <0.0982 0.976 0.7621 mg/Kg 78 39 -150 12 40 p-Isopropyltoluene 0.480 0.976 1.169 mg/Kg 71 42 -150 12 36 Methyl ethyl ketone (MEK)<0.736 1.95 1.804 mg/Kg 92 36 -150 2 40 4-Methyl-2-pentanone (MIBK)<0.0982 1.95 1.985 mg/Kg 97 44 -150 0 40 Methyl tert-butyl ether <0.0982 0.976 0.8489 mg/Kg 87 52 -150 1 33 Naphthalene <0.245 0.976 0.9040 mg/Kg 79 19 -150 0 40 Propylbenzene, n-<0.0982 0.976 0.7738 mg/Kg 79 33 -150 12 40 Styrene <0.0982 0.976 0.7770 mg/Kg 80 44 -150 3 38 1,1,1,2-Tetrachloroethane <0.0982 0.976 0.7997 mg/Kg 82 43 -150 2 35 1,1,2,2-Tetrachloroethane <0.0982 0.976 0.9496 mg/Kg 97 45 -150 6 40 Tetrachloroethene <0.0982 0.976 0.6516 mg/Kg 67 44 -150 14 40 Tetrahydrofuran <0.0982 1.95 1.813 mg/Kg 93 42 -150 12 40 Toluene <0.0982 0.976 0.8206 mg/Kg 84 49 -150 20 39 1,2,3-Trichlorobenzene <0.0982 0.976 0.5860 mg/Kg 60 37 -150 5 35 1,2,4-Trichlorobenzene <0.0982 0.976 0.6167 mg/Kg 63 37 -150 6 40 1,1,1-Trichloroethane <0.0982 0.976 0.9240 mg/Kg 95 50 -150 2 36 1,1,2-Trichloroethane <0.0982 0.976 0.9238 mg/Kg 95 59 -150 4 39 Trichloroethene <0.0982 0.976 0.8342 mg/Kg 85 53 -150 4 35 1,2,3-Trichloropropane <0.0982 0.976 0.8675 mg/Kg 89 48 -150 7 40 1,1,2-Trichlorotrifluoroethane <0.0982 0.976 0.9148 mg/Kg 94 44 -150 2 35 1,2,4-Trimethylbenzene 0.259 0.976 0.9500 mg/Kg 71 28 -150 2 40 1,3,5-Trimethylbenzene 0.146 0.976 0.8054 mg/Kg 67 32 -150 5 40 Xylenes, Total <0.147 1.95 1.774 mg/Kg 84 36 -150 3 40 4-Bromofluorobenzene (Surr)79 -120 Surrogate 107 MSD MSD Qualifier Limits%Recovery 95Dibromofluoromethane (Surr)80 -124 101Toluene-d8 (Surr)78 -120 Client Sample ID: Method BlankLab Sample ID: MB 310-351186/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 351296 Prep Batch: 351186 RL MDL Acetone <0.482 0.482 mg/Kg 04/27/22 09:42 04/27/22 14:05 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier <0.0964 0.0964 mg/Kg 04/27/22 09:42 04/27/22 14:05 1Allyl chloride Eurofins Cedar Falls Page 46 of 90 5/17/2022 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15