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QC Sample Results Job ID: 310-229849-1Client: WSB & Associates, Inc Project/Site: Kenzie Terrace Method: 8260D - Volatile Organic Compounds by GC/MS (Continued) Client Sample ID: Matrix SpikeLab Sample ID: 310-229836-A-6-B MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 351296 Prep Batch: 351186 Acetone <0.439 1.98 1.475 mg/Kg 74 30 -150 Analyte MS MS DUnitResultQualifier %Rec Spike Added Sample Result Sample Qualifier %Rec Limits Allyl chloride <0.0877 0.991 0.6940 mg/Kg 70 46 -150 Benzene 0.571 F1 0.991 0.9489 F1 mg/Kg 38 49 -150 Bromobenzene <0.0877 0.991 0.6088 mg/Kg 61 49 -150 Bromochloromethane <0.0877 0.991 0.7216 mg/Kg 73 48 -150 Bromodichloromethane <0.0877 0.991 0.7132 mg/Kg 72 45 -150 Bromoform <0.0877 0.991 0.5046 mg/Kg 51 32 -150 Butylbenzene, n-<0.0877 0.991 0.6177 mg/Kg 62 21 -150 Butylbenzene, sec-<0.0877 0.991 0.5887 mg/Kg 59 35 -150 Butylbenzene, tert-<0.0877 0.991 0.5921 mg/Kg 60 49 -150 Carbon tetrachloride <0.0877 0.991 0.7227 mg/Kg 73 43 -150 Chlorobenzene <0.0877 0.991 0.6603 mg/Kg 67 50 -150 Chloroform <0.0877 0.991 0.7595 mg/Kg 77 51 -150 2-Chlorotoluene <0.0877 0.991 0.6887 mg/Kg 69 36 -150 4-Chlorotoluene <0.0877 0.991 0.6536 mg/Kg 66 40 -150 Dibromo-3-chloropropane, 1,2-<0.0877 0.991 0.5429 mg/Kg 55 33 -150 Dibromochloromethane <0.0877 0.991 0.5739 mg/Kg 58 41 -150 Dibromoethane, 1,2-<0.0877 0.991 0.7000 mg/Kg 71 52 -150 Dibromomethane <0.0877 0.991 0.6731 mg/Kg 68 51 -150 Dichlorobenzene, 1,2-<0.0877 0.991 0.5799 mg/Kg 59 45 -150 Dichlorobenzene, 1,3-<0.0877 0.991 0.5883 mg/Kg 59 47 -150 Dichlorobenzene, 1,4-<0.0877 0.991 0.5724 mg/Kg 58 46 -150 Dichloroethane, 1,1-<0.0877 0.991 0.7260 mg/Kg 73 54 -150 Dichloroethane, 1,2-<0.0877 0.991 0.8161 mg/Kg 82 54 -150 Dichloroethylene, 1,1-<0.0877 0.991 0.6216 mg/Kg 63 44 -150 Dichloroethylene, cis-1,2-<0.0877 0.991 0.6585 mg/Kg 66 53 -150 Dichloroethylene, trans-1,2 <0.0877 0.991 0.6336 mg/Kg 64 52 -150 Dichloromethane <0.219 0.991 0.6528 mg/Kg 66 47 -150 Dichloropropane, 1,2-<0.0877 0.991 0.7795 mg/Kg 79 52 -150 Dichloropropane, 1,3-<0.0877 0.991 0.7381 mg/Kg 74 54 -150 Dichloropropane, 2,2-<0.0877 0.991 0.6597 mg/Kg 67 34 -150 Dichloropropene, 1,1-<0.0877 0.991 0.7653 mg/Kg 77 52 -150 Dichloropropene, cis 1,3-<0.0877 0.991 0.7023 mg/Kg 71 46 -150 Dichloropropene, trans 1,3-<0.0877 0.991 0.6993 mg/Kg 71 48 -150 Ethyl ether <0.0877 0.991 0.6694 mg/Kg 68 51 -150 Ethylbenzene <0.0877 0.991 0.7355 mg/Kg 71 34 -150 Hexachlorobutadiene <0.0877 0.991 0.5205 mg/Kg 53 22 -150 Isopropylbenzene <0.0877 0.991 0.6562 mg/Kg 66 39 -150 p-Isopropyltoluene <0.0877 0.991 0.5594 mg/Kg 56 42 -150 Methyl ethyl ketone (MEK)<0.658 1.98 1.314 mg/Kg 66 36 -150 4-Methyl-2-pentanone (MIBK)<0.0877 1.98 1.423 mg/Kg 72 44 -150 Methyl tert-butyl ether <0.0877 0.991 0.6716 mg/Kg 68 52 -150 Naphthalene <0.219 0.991 0.6007 mg/Kg 61 19 -150 Propylbenzene, n-<0.0877 0.991 0.6886 mg/Kg 69 33 -150 Styrene <0.0877 0.991 0.6137 mg/Kg 62 44 -150 1,1,1,2-Tetrachloroethane <0.0877 0.991 0.6409 mg/Kg 65 43 -150 1,1,2,2-Tetrachloroethane <0.0877 0.991 0.6712 mg/Kg 68 45 -150 Tetrachloroethene <0.0877 0.991 0.6258 mg/Kg 63 44 -150 Eurofins Cedar Falls Page 50 of 90 5/17/2022 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15