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QC Sample Results Job ID: 310-229849-1Client: WSB & Associates, Inc Project/Site: Kenzie Terrace Method: 8260D - Volatile Organic Compounds by GC/MS (Continued) Client Sample ID: Matrix Spike DuplicateLab Sample ID: 310-229836-A-6-C MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 351296 Prep Batch: 351186 Dichloroethylene, cis-1,2-<0.0877 0.988 0.7013 mg/Kg 71 53 -150 6 37 Analyte MSD MSD DUnitResultQualifier %Rec Spike Added Sample Result Sample Qualifier %Rec Limits LimitRPD RPD Dichloroethylene, trans-1,2 <0.0877 0.988 0.6725 mg/Kg 68 52 -150 6 33 Dichloromethane <0.219 0.988 0.6912 mg/Kg 70 47 -150 6 32 Dichloropropane, 1,2-<0.0877 0.988 0.7453 mg/Kg 75 52 -150 4 38 Dichloropropane, 1,3-<0.0877 0.988 0.7532 mg/Kg 76 54 -150 2 37 Dichloropropane, 2,2-<0.0877 0.988 0.6637 mg/Kg 67 34 -150 1 33 Dichloropropene, 1,1-<0.0877 0.988 0.7707 mg/Kg 78 52 -150 1 38 Dichloropropene, cis 1,3-<0.0877 0.988 0.6851 mg/Kg 69 46 -150 2 39 Dichloropropene, trans 1,3-<0.0877 0.988 0.7138 mg/Kg 72 48 -150 2 39 Ethyl ether <0.0877 0.988 0.6783 mg/Kg 69 51 -150 1 35 Ethylbenzene <0.0877 0.988 0.6723 mg/Kg 65 34 -150 9 39 Hexachlorobutadiene <0.0877 0.988 0.5341 mg/Kg 54 22 -150 3 40 Isopropylbenzene <0.0877 0.988 0.6346 mg/Kg 64 39 -150 3 40 p-Isopropyltoluene <0.0877 0.988 0.5666 mg/Kg 57 42 -150 1 36 Methyl ethyl ketone (MEK)<0.658 1.98 1.381 mg/Kg 70 36 -150 5 40 4-Methyl-2-pentanone (MIBK)<0.0877 1.98 1.361 mg/Kg 69 44 -150 4 40 Methyl tert-butyl ether <0.0877 0.988 0.6739 mg/Kg 68 52 -150 0 33 Naphthalene <0.219 0.988 0.6044 mg/Kg 61 19 -150 1 40 Propylbenzene, n-<0.0877 0.988 0.6375 mg/Kg 65 33 -150 8 40 Styrene <0.0877 0.988 0.6075 mg/Kg 62 44 -150 1 38 1,1,1,2-Tetrachloroethane <0.0877 0.988 0.6149 mg/Kg 62 43 -150 4 35 1,1,2,2-Tetrachloroethane <0.0877 0.988 0.6768 mg/Kg 69 45 -150 1 40 Tetrachloroethene <0.0877 0.988 0.5981 mg/Kg 61 44 -150 5 40 Tetrahydrofuran <0.0877 1.98 1.353 mg/Kg 69 42 -150 6 40 Toluene <0.0877 F2 0.988 0.6717 F2 mg/Kg 68 49 -150 45 39 1,2,3-Trichlorobenzene <0.0877 0.988 0.5008 mg/Kg 51 37 -150 1 35 1,2,4-Trichlorobenzene <0.0877 0.988 0.5324 mg/Kg 54 37 -150 4 40 1,1,1-Trichloroethane <0.0877 0.988 0.7230 mg/Kg 73 50 -150 1 36 1,1,2-Trichloroethane <0.0877 0.988 0.7091 mg/Kg 72 59 -150 3 39 Trichloroethene <0.0877 0.988 0.7238 mg/Kg 73 53 -150 3 35 1,2,3-Trichloropropane <0.0877 0.988 0.6495 mg/Kg 66 48 -150 3 40 1,1,2-Trichlorotrifluoroethane <0.0877 0.988 0.6918 mg/Kg 70 44 -150 3 35 1,2,4-Trimethylbenzene <0.0877 0.988 0.6720 mg/Kg 68 28 -150 35 40 1,3,5-Trimethylbenzene <0.0877 0.988 0.6385 mg/Kg 65 32 -150 12 40 Xylenes, Total <0.132 1.98 1.306 mg/Kg 66 36 -150 13 40 4-Bromofluorobenzene (Surr)79 -120 Surrogate 101 MSD MSD Qualifier Limits%Recovery 104Dibromofluoromethane (Surr)80 -124 101Toluene-d8 (Surr)78 -120 Client Sample ID: Method BlankLab Sample ID: MB 310-351205/5 Matrix: Water Prep Type: Total/NA Analysis Batch: 351205 RL MDL Acetone <10.0 10.0 ug/L 04/27/22 11:30 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier <2.00 2.00 ug/L 04/27/22 11:30 1Allyl chloride Eurofins Cedar Falls Page 52 of 90 5/17/2022 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15