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(1) Where applicable, custom lab flags have been used on this report; U = not detected at RL; B = analyte found in the associated blank and concentration in <br />sample is less than 10X the concentration in the associated blank; J = concentration less than limit of quantification. <br />(2) Reporting Limit (Code): S = sample detection limit; M = method detection limit; L = lowest calibration level equivalent; Q = minimum reporting level. <br />These data are validated and reported as accurate and in accord with SGS AXYS Analytical Services Ltd. ISO17025 compliant quality assurance processes. <br />Signed: ___________Bryan Alonzo___________ <br />For Axys Internal Use Only [ XSL Template: FC-Form1A.xsl; Created: 16-Jun-2020 11:23:07; Application: XMLTransformer-1.18.7; <br />Report Filename: PFC_FC_LC_PFAS_L33032-1_Form1A_FC0L_151S20_SJ2745753.html; Workgroup: WG72387; Design ID: 3973 ] <br />SGS AXYS METHOD MLA-110 Rev 02 CLIENT SAMPLE NO. <br />Lino Lakes Well No.4 <br />Sample Collection: <br />05-May-2020 10:30 <br />Form 1A <br />PERFLUORINATED ORGANICS ANALYSIS REPORT <br />SGS AXYS ANALYTICAL SERVICES <br />2045 MILLS RD., SIDNEY, B.C., CANADA <br />V8L 5X2 TEL (250) 655-5800 FAX (250) 655-5811 <br />Project No.LINO LAKES WTP FEASIBILITY <br />015822-000 <br />Contract No.:5036 Lab Sample I.D.:L33032-1 <br />Matrix:AQUEOUS Sample Size:0.547 L <br />Sample Receipt Date:06-May-2020 Initial Calibration Date:18-Mar-2020 <br />Extraction Date:15-May-2020 Instrument ID:LCMS/MS <br />Analysis Date:15-May-2020 Time:21:27:16 Column ID:C18 <br />Extract Volume (uL):4000 Sample Data Filename:FC0L_151 S: 20 <br />Injection Volume (uL):2 Blank Data Filename:FC0L_151 S: 19 <br />Dilution Factor:N/A Cal. Ver. Data Filename:FC0L_151 S: 12 <br />Concentration Units:ng/L <br />This page is part of a total report that contains information necessary for accreditation compliance. <br />Results are compliant with NELAP accreditation described in the total report. Sample results relate only to the sample tested. <br />COMPOUND LAB FLAG 1 CONC. <br />FOUND <br />REPORTING <br />LIMIT (RL)2 <br />RETENTION <br />TIME <br />PFBA U 2.92 (L) <br />PFPeA U 1.46 (L) <br />PFHxA U 0.731 (L) <br />PFHpA U 0.731 (L) <br />PFOA U 0.731 (L) <br />PFNA U 0.731 (L) <br />PFDA U 0.731 (L) <br />PFUnA U 0.731 (L) <br />PFDoA U 0.731 (L) <br />PFTrDA U 0.731 (L) <br />PFTeDA U 0.731 (L) <br />PFBS U 0.731 (L) <br />PFPeS U 0.731 (L) <br />PFHxS U 0.731 (L) <br />PFHpS U 0.731 (L) <br />PFOS U 0.731 (L) <br />PFNS U 0.731 (L) <br />PFDS U 0.731 (L) <br />PFDoS U 0.731 (L) <br />4:2 FTS U 2.92 (L) <br />6:2 FTS B J 5.45 2.63 (L)5:51 <br />8:2 FTS U 2.92 (L) <br />PFOSA U 0.731 (L) <br />N-MeFOSA U 0.840 (L) <br />N-EtFOSA U 1.83 (L) <br />MeFOSAA U 0.731 (L) <br />EtFOSAA U 0.731 (L) <br />N-MeFOSE U 7.31 (L) <br />N-EtFOSE U 5.48 (L) <br />HFPO-DA U 2.78 (L) <br />ADONA U 2.92 (L) <br />9Cl-PF3ONS U 2.92 (L) <br />11Cl-PF3OUdS U 2.92 (L) <br />Page 1 of 1 (WG72387 -PFC_FC_LC_PFAS_L33032-1_Form1A_FC0L_151S20_SJ2745753.html) <br />www.axysanalytical.com <br />Page 36 of 94