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(1) Where applicable, custom lab flags have been used on this report. <br />(2) R(%) = percent recovery. <br />These data are validated and reported as accurate and in accord with SGS AXYS Analytical Services Ltd. ISO17025 compliant quality assurance <br />processes. <br />Signed: ___________Bryan Alonzo___________ <br />For Axys Internal Use Only [ XSL Template: FC-Form2.xsl; Created: 16-Jun-2020 11:23:07; Application: XMLTransformer-1.18.7; <br />Report Filename: PFC_FC_LC_PFAS_L33032-1_Form2_FC0L_151S20_SJ2745753.html; Workgroup: WG72387; Design ID: 3973 ] <br />SGS AXYS METHOD MLA-110 Rev 02 CLIENT SAMPLE NO. <br />Lino Lakes Well No.4 <br />Sample Collection: <br />05-May-2020 10:30 <br />Form 2 <br />PERFLUORINATED ORGANICS ANALYSIS REPORT <br />SGS AXYS ANALYTICAL SERVICES <br />2045 MILLS RD., SIDNEY, B.C., CANADA <br />V8L 5X2 TEL (250) 655-5800 FAX (250) 655-5811 <br />Project No.LINO LAKES WTP FEASIBILITY <br />015822-000 <br />Contract No.:5036 Lab Sample I.D.:L33032-1 <br />Matrix:AQUEOUS Sample Size:0.547 L <br />Sample Receipt Date:06-May-2020 Initial Calibration Date:18-Mar-2020 <br />Extraction Date:15-May-2020 Instrument ID:LCMS/MS <br />Analysis Date:15-May-2020 Time:21:27:16 Column ID:C18 <br />Extract Volume (uL):4000 Sample Data Filename:FC0L_151 S: 20 <br />Injection Volume (uL):2 Blank Data Filename:FC0L_151 S: 19 <br />Dilution Factor:N/A Cal. Ver. Data Filename:FC0L_151 S: 12 <br />Concentration Units:ng absolute <br />This page is part of a total report that contains information necessary for accreditation compliance. <br />Results are compliant with NELAP accreditation described in the total report. Sample results relate only to the sample tested. <br />LABELED COMPOUND LAB <br />FLAG 1 <br />SPIKE <br />CONC. <br />CONC. <br />FOUND R(%)2 RETENTION <br />TIME <br />13C4-PFBA 40.0 33.0 82.5 1:55 <br />13C5-PFPeA 20.0 17.6 88.2 4:21 <br />13C5-PFHxA 10.0 8.63 86.3 4:56 <br />13C4-PFHpA 10.0 9.14 91.4 5:24 <br />13C8-PFOA 10.0 8.50 85.0 6:10 <br />13C9-PFNA 5.00 3.92 78.4 7:01 <br />13C6-PFDA 5.00 4.60 92.1 7:30 <br />13C7-PFUnA 5.00 4.27 85.5 7:50 <br />13C2-PFDoA 5.00 4.16 83.2 8:06 <br />13C2-PFTeDA 5.00 3.74 74.8 8:52 <br />13C3-PFBS 10.0 8.43 84.3 4:53 <br />13C3-PFHxS 10.0 8.37 83.7 6:17 <br />13C8-PFOS 10.0 8.83 88.3 7:36 <br />13C2-4:2 FTS 20.0 12.7 63.5 4:49 <br />13C2-6:2 FTS 20.0 12.5 62.3 5:51 <br />13C2-8:2 FTS 20.0 13.1 65.6 7:21 <br />13C8-PFOSA 10.0 8.75 87.5 8:43 <br />D3-N-MeFOSA 10.0 7.76 77.6 10:07 <br />D5-N-EtFOSA 10.0 6.93 69.3 10:24 <br />D3-MeFOSAA 20.0 11.2 56.0 7:33 <br />D5-EtFOSAA 20.0 10.6 52.9 7:42 <br />d7-NMe-FOSE 100 69.9 69.9 9:59 <br />d9-NEt-FOSE 100 63.6 63.6 10:17 <br />13C3-HFPO-DA 40.0 31.9 79.8 5:04 <br />Page 1 of 1 (WG72387 -PFC_FC_LC_PFAS_L33032-1_Form2_FC0L_151S20_SJ2745753.html) <br />www.axysanalytical.com <br />Page 37 of 94