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(1) Where applicable, custom lab flags have been used on this report. <br />These data are validated and reported as accurate and in accord with SGS AXYS Analytical Services Ltd. ISO17025 compliant quality assurance <br />processes. <br />Signed: ___________Jordan Berends___________ <br />For Axys Internal Use Only [ XSL Template: FC-Form3B.xsl; Created: 16-Jun-2020 11:23:07; Application: XMLTransformer-1.18.7; <br />Report Filename: PFOA_FC_LC_18-Mar-2020_FC0L__Form3B_GS87543.html; Workgroup: WG72387; Design ID: 3973 ] <br />SGS AXYS METHOD MLA-110 Rev 02 <br />Form 3B <br />LC MS/MS INITIAL CALIBRATION PERCENT RECOVERIES <br />SGS AXYS ANALYTICAL SERVICES <br />2045 MILLS RD., SIDNEY, B.C., CANADA <br />V8L 5X2 TEL (250) 655-5800 FAX (250) 655-5811 <br />CS0 Data Filename:N/A <br />Initial Calibration Date:18-Mar-2020 CS1 Data Filename:FC0L_082 S: 10 <br />Instrument ID:LC MS/MS CS2 Data Filename:FC0L_082 S: 11 <br />LC Column ID:C18 CS3 Data Filename:FC0L_082 S: 12 <br />CS4 Data Filename:FC0L_082 S: 13 <br />CS5 Data Filename:FC0L_082 S: 14 <br />CS6 Data Filename:FC0L_082 S: 15 <br />CS7 Data Filename:FC0L_082 S: 16 <br />CS8 Data Filename:N/A <br />PERCENT RECOVERIES (%) <br />CS0 CS1 CS2 CS3 CS4 CS5 CS6 CS7 CS8 <br />LABELED COMPOUND LAB <br />FLAG 1 <br />13C4-PFBA 99.0 102 99.9 99.7 100 99.5 99.1 <br />13C5-PFPeA 108 106 104 105 103 94.5 79.2 <br />13C5-PFHxA 102 103 99.3 101 102 99.2 94.1 <br />13C4-PFHpA 95.2 106 105 106 106 94.9 86.8 <br />13C8-PFOA 97.0 101 103 101 106 95.5 95.7 <br />13C9-PFNA 97.7 105 104 99.3 97.3 102 95.1 <br />13C6-PFDA 114 108 82.8 113 106 98.3 77.0 <br />13C7-PFUnA 114 118 103 103 93.3 67.7 <br />13C2-PFDoA 111 111 96.0 85.8 98.6 94.8 103 <br />13C2-PFTeDA 97.0 102 95.6 94.2 94.1 99.3 118 <br />13C3-PFBS 97.7 112 105 102 101 99.2 82.6 <br />13C3-PFHxS 101 104 102 99.9 101 101 91.4 <br />13C8-PFOS 99.7 88.7 104 104 100 105 98.6 <br />13C2-4:2 FTS 105 116 109 96.6 73.2 <br />13C2-6:2 FTS 105 116 115 106 88.3 70.0 <br />13C2-8:2 FTS 111 116 116 114 85.5 71.7 85.6 <br />13C8-PFOSA 92.4 95.4 90.5 92.6 90.8 104 134 <br />D3-N-MeFOSA 97.8 101 88.3 95.5 100 118 <br />D5-N-EtFOSA 97.3 96.0 91.1 95.6 90.7 107 122 <br />D3-MeFOSAA 96.2 92.6 97.5 93.6 95.9 103 121 <br />D5-EtFOSAA 97.5 100 93.2 97.7 96.2 109 106 <br />d7-NMe-FOSE 95.8 95.8 89.7 96.2 95.8 107 120 <br />d9-NEt-FOSE 95.6 98.2 88.6 95.4 93.9 105 124 <br />13C3-HFPO-DA 109 110 110 107 101 90.0 72.7 <br />Page 1 of 1 (WG72387 -PFOA_FC_LC_18-Mar-2020_FC0L__Form3B_GS87543.html) <br />www.axysanalytical.com <br />Page 54 of 94