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(1) Where applicable, custom lab flags have been used on this report. <br />These data are validated and reported as accurate and in accord with SGS AXYS Analytical Services Ltd. ISO17025 compliant quality assurance processes. <br />Signed: ___________Jordan Berends___________ <br />For Axys Internal Use Only [ XSL Template: FC-Form3C.xsl; Created: 16-Jun-2020 11:23:07; Application: XMLTransformer-1.18.7; <br />Report Filename: PFOA_FC_LC_18-Mar-2020_FC0L__Form3C_GS87543.html; Workgroup: WG72387; Design ID: 3973 ] <br />SGS AXYS METHOD MLA-110 Rev 02 <br />Form 3C <br />LC MS/MS INITIAL CALIBRATION RETENTION TIMES <br />SGS AXYS ANALYTICAL SERVICES <br />2045 MILLS RD., SIDNEY, B.C., CANADA <br />V8L 5X2 TEL (250) 655-5800 FAX (250) 655-5811 <br />CS0 Data Filename:N/A <br />Initial Calibration Date:18-Mar-2020 CS1 Data Filename:FC0L_082 S: 10 <br />Instrument ID:LC MS/MS CS2 Data Filename:FC0L_082 S: 11 <br />LC Column ID:C18 CS3 Data Filename:FC0L_082 S: 12 <br />CS4 Data Filename:FC0L_082 S: 13 <br />CS5 Data Filename:FC0L_082 S: 14 <br />CS6 Data Filename:FC0L_082 S: 15 <br />CS7 Data Filename:FC0L_082 S: 16 <br />CS8 Data Filename:N/A <br />RETENTION TIMES <br />CS0 CS1 CS2 CS3 CS4 CS5 CS6 CS7 CS8 MEAN <br />RT <br />COMPOUND LAB <br />FLAG 1 <br />PFBA 1:58 1:58 1:58 1:58 1:58 1:58 1:58 1:58 <br />PFPeA 4:19 4:19 4:19 4:19 4:19 4:19 4:19 4:19 <br />PFHxA 4:54 4:54 4:53 4:53 4:54 4:54 4:54 4:54 <br />PFHpA 5:23 5:23 5:23 5:23 5:23 5:23 5:24 5:23 <br />PFOA 6:11 6:11 6:11 6:11 6:11 6:11 6:11 6:11 <br />PFNA 7:02 7:03 7:02 7:03 7:02 7:02 7:02 7:02 <br />PFDA 7:34 7:34 7:33 7:34 7:33 7:34 7:33 7:34 <br />PFUnA 7:54 7:54 7:53 7:54 7:54 7:54 7:54 7:54 <br />PFDoA 8:10 8:10 8:10 8:10 8:10 8:10 8:10 8:10 <br />PFTrDA 8:30 8:30 8:29 8:29 8:30 8:30 8:30 <br />PFTeDA 8:55 8:55 8:55 8:55 8:55 8:55 8:55 8:55 <br />PFBS 4:51 4:51 4:51 4:51 4:51 4:51 4:51 4:51 <br />PFPeS 5:25 5:26 5:25 5:25 5:25 5:26 5:26 5:25 <br />PFHxS 6:17 6:17 6:17 6:17 6:17 6:17 6:17 6:17 <br />PFHpS 7:09 7:09 7:09 7:09 7:09 7:09 7:09 7:09 <br />PFOS 7:40 7:40 7:39 7:40 7:39 7:40 7:39 7:40 <br />PFNS 7:59 7:59 7:59 7:59 7:59 7:59 7:59 7:59 <br />PFDS 8:16 8:16 8:16 8:16 8:16 8:16 8:16 8:16 <br />PFDoS 9:06 9:06 9:06 9:06 9:06 9:06 9:06 9:06 <br />4:2 FTS 4:46 4:46 4:46 4:46 4:46 4:46 4:46 4:46 <br />6:2 FTS 5:51 5:51 5:51 5:51 5:51 5:51 5:51 <br />8:2 FTS 7:24 7:23 7:23 7:23 7:23 7:23 7:23 <br />PFOSA 8:45 8:45 8:45 8:45 8:45 8:45 8:45 8:45 <br />N-MeFOSA 10:12 10:12 10:12 10:12 10:12 10:12 10:12 10:12 <br />N-EtFOSA 10:30 10:30 10:31 10:30 10:30 10:30 10:30 10:30 <br />MeFOSAA 7:37 7:37 7:37 7:37 7:37 7:37 7:37 7:37 <br />EtFOSAA 7:46 7:46 7:45 7:46 7:45 7:46 7:45 7:46 <br />N-MeFOSE 10:04 10:03 10:04 10:04 10:04 10:04 10:04 10:04 <br />N-EtFOSE 10:23 10:23 10:23 10:23 10:23 10:23 10:23 10:23 <br />HFPO-DA 5:03 5:03 5:03 5:03 5:03 5:03 5:03 5:03 <br />ADONA 5:38 5:38 5:38 5:38 5:38 5:38 5:38 5:38 <br />9Cl-PF3ONS 7:54 7:54 7:53 7:53 7:53 7:54 7:53 7:53 <br />11Cl-PF3OUdS 8:31 8:31 8:31 8:31 8:31 8:31 8:31 8:31 <br />Page 1 of 1 (WG72387 -PFOA_FC_LC_18-Mar-2020_FC0L__Form3C_GS87543.html) <br />www.axysanalytical.com <br />Page 55 of 94