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QC Sample Results <br />Job ID: 310-229849-1Client: WSB & Associates, Inc <br />Project/Site: Kenzie Terrace <br />Method: 8260D - Volatile Organic Compounds by GC/MS (Continued) <br />Client Sample ID: Matrix SpikeLab Sample ID: 310-229814-B-22 MS <br />Matrix: Water Prep Type: Total/NA <br />Analysis Batch: 351205 <br />Dichloropropane, 2,2-<4.00 25.0 19.35 ug/L 77 20 -150 <br />Analyte <br />MS MS <br />DUnitResultQualifier %Rec <br />Spike <br />Added <br />Sample <br />Result <br />Sample <br />Qualifier <br />%Rec <br />Limits <br />Dichloropropene, 1,1-<1.00 25.0 21.38 ug/L 86 51 -130 <br />Dichloropropene, cis 1,3-<5.00 25.0 22.46 ug/L 90 45 -131 <br />Dichloropropene, trans 1,3-<5.00 25.0 21.62 ug/L 86 43 -133 <br />Diethyl ether <2.00 25.0 21.41 ug/L 81 57 -134 <br />Ethylbenzene <1.00 25.0 23.42 ug/L 94 40 -138 <br />Hexachlorobutadiene <5.00 25.0 19.41 ug/L 78 19 -150 <br />Isopropylbenzene <1.00 25.0 22.95 ug/L 92 42 -132 <br />p-Isopropyltoluene <1.00 25.0 23.12 ug/L 92 35 -134 <br />Methyl ethyl ketone (MEK)<10.0 50.0 53.26 ug/L 107 47 -150 <br />4-Methyl-2-pentanone (MIBK)<10.0 50.0 54.88 ug/L 110 51 -144 <br />Methyl tert-butyl ether <1.00 25.0 24.93 ug/L 97 56 -132 <br />Naphthalene <5.00 25.0 23.61 ug/L 94 37 -150 <br />Propylbenzene, n-<1.00 25.0 22.97 ug/L 92 37 -135 <br />Styrene <1.00 25.0 23.22 ug/L 93 44 -138 <br />1,1,1,2-Tetrachloroethane <1.00 25.0 23.53 ug/L 94 45 -140 <br />1,1,2,2-Tetrachloroethane <1.00 25.0 23.97 ug/L 96 51 -140 <br />Tetrachloroethene <1.00 25.0 19.87 ug/L 79 43 -135 <br />Tetrahydrofuran <10.0 50.0 54.68 ug/L 109 44 -150 <br />Toluene <1.00 25.0 21.82 ug/L 87 44 -136 <br />1,2,3-Trichlorobenzene <5.00 25.0 22.15 ug/L 89 37 -150 <br />1,2,4-Trichlorobenzene <5.00 25.0 21.22 ug/L 85 38 -135 <br />1,1,1-Trichloroethane <1.00 25.0 21.53 ug/L 86 52 -129 <br />1,1,2-Trichloroethane <1.00 25.0 23.05 ug/L 92 50 -142 <br />Trichloroethene <1.00 25.0 22.47 ug/L 90 49 -130 <br />1,2,3-Trichloropropane <1.00 25.0 23.47 ug/L 94 49 -146 <br />1,1,2-Trichlorotrifluoroethane <2.00 25.0 15.16 ug/L 61 42 -142 <br />1,2,4-Trimethylbenzene <1.00 25.0 22.91 ug/L 92 37 -142 <br />1,3,5-Trimethylbenzene <1.00 25.0 23.09 ug/L 92 39 -142 <br />Xylenes, Total <3.00 50.0 49.39 ug/L 99 40 -140 <br />4-Bromofluorobenzene (Surr)80 -120 <br />Surrogate <br />97 <br />MS MS <br />Qualifier Limits%Recovery <br />100Dibromofluoromethane (Surr)79 -120 <br />104Toluene-d8 (Surr)79 -120 <br />Client Sample ID: Matrix Spike DuplicateLab Sample ID: 310-229814-B-22 MSD <br />Matrix: Water Prep Type: Total/NA <br />Analysis Batch: 351205 <br />Acetone <10.0 50.0 52.27 ug/L 105 37 -150 5 29 <br />Analyte <br />MSD MSD <br />DUnitResultQualifier %Rec <br />Spike <br />Added <br />Sample <br />Result <br />Sample <br />Qualifier <br />%Rec <br />Limits LimitRPD <br />RPD <br />Allyl chloride <2.00 25.0 20.37 ug/L 81 38 -150 6 32 <br />Benzene <0.500 25.0 21.61 ug/L 86 54 -128 8 21 <br />Bromobenzene <1.00 25.0 23.15 ug/L 93 47 -139 6 23 <br />Bromochloromethane <5.00 25.0 20.82 ug/L 83 63 -143 5 24 <br />Bromodichloromethane <1.00 25.0 22.79 ug/L 91 50 -135 3 24 <br />Bromoform <5.00 25.0 21.31 ug/L 85 40 -139 1 22 <br />Eurofins Cedar Falls <br />Page 57 of 90 5/17/2022 <br />1 <br />2 <br />3 <br />4 <br />5 <br />6 <br />7 <br />8 <br />9 <br />10 <br />11 <br />12 <br />13 <br />14 <br />15